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classificationIPCAdditional http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C12R1-645
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07J63-00
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C12P33-00
filingDate 2013-06-25^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2014-10-29^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2014-10-29^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-103305582-B
titleOfInvention Method for extracting 17(21)-hopene-12beta-diol out of aschersonia
abstract The invention discloses a method for extracting 17(21)-hopene-12beta-diol out of aschersonia. The method comprises the following steps of: extracting, separating and purifying metabolite, namely, extracting in a quenching mode, concentrating so as to obtain a crude extract, passing the crude extract through a silica gel column of 160-200 meshes, carrying out gradient elution by using n-hexane and ethyl acetate, further passing through a silica gel column of 200-300 meshes, carrying out gradient elution by using petroleum ether and ethyl acetate, and finally recrystallizing so as to obtain the 17(21)-hopene-12beta-diol in the aschersonia. The method is simple in process, easy to operate, low in cost and high in purity; and materials are conveniently obtained.
priorityDate 2013-06-25^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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