http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104628892-B
Outgoing Links
| Predicate | Object |
|---|---|
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08B37-16 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01D15-22 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J20-29 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J20-30 |
| filingDate | 2015-01-23^^<http://www.w3.org/2001/XMLSchema#date> |
| grantDate | 2017-02-22^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationDate | 2017-02-22^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-104628892-B |
| titleOfInvention | Preparation method and use of 6-benzyl phenylethylamine derivative beta-cyclodextrin bonded SBA-15 |
| abstract | The invention discloses a preparation method of 6-benzyl phenylethylamine derivative beta-cyclodextrin bonded SBA-15. The preparation method comprises the following steps: with 6-p-tolylsulfonyl beta-cyclodextrin and N-benzyl-1-phenylethylamine as raw materials, preparing a 6-benzyl phenylethylamine derivative beta-cyclodextrin ligand; adding a coupling agent 3-isocyanate propyl siloxane, and reacting to prepare siloxane containing the 6-benzyl phenylethylamine derivative beta-cyclodextrin; with an ordered mesoporous SBA-15 silica gel as a bonding matrix, reacting the bonding matrix with the siloxane containing the 6-benzyl phenylethylamine derivative beta-cyclodextrin to obtain a coarse product of 6-benzyl phenylethylamine derivative beta-cyclodextrin bonded SBA-15; with acetone as a solvent, extracting and purifying via a soxhlet to prepare the 6-benzyl phenylethylamine derivative beta-cyclodextrin bonded SBA-15. The preparation method disclosed by the invention is simple and the convenient, the cost is lower, the adaptability is wide, the stereoselectivity is stronger, meanwhile the permeability is good, the mass transfer resistance is small, and the 6-benzyl phenylethylamine derivative beta-cyclodextrin bonded SBA-15 can be used as a stationary phase in chiral chromatography for the chiral separation and analysis of high performance Liquid chromatography. |
| priorityDate | 2015-01-23^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
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