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filingDate 2014-01-13^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2017-03-29^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2017-03-29^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-104936930-B
titleOfInvention The method that the oxidative dehydrogenation of n-butene prepares butadiene is carried out by peroxide content is monitored during product is processed
abstract The present invention relates to the method for preparing butadiene from n-butene, including:A feed gas stream (a) containing n-butene are provided);B stream (a) and oxygen-containing gas are introduced into dehydrogenation zone and by n-butene oxidative dehydrogenation into butadiene), product gas stream (b) are obtained;C) stream (b) is cooled down and is compressed, stream (b) is contacted with coolant and obtain condensate stream (c1) and the gas streams containing butadiene, n-butene, vapor, oxygen and low boiling hydrocarbon (c2);D C is absorbed in absorbing medium) 4 Hydrocarbon is separating low-boiling point gas composition, the medium stream that is absorbed and gas streams (d2), from absorbing medium stream desorbing C from stream (c2) 4 Hydrocarbon obtains C 4 Product gas stream (d1);E stream (d1) extractive distillation is separated into into the stream containing butadiene (e1) and the stream containing n-butene (e2));F stream (e1) distillation is obtained into stream (f1) and the stream containing butadiene (f2));Wherein in step C) in the coolant supplied from loop and/or in step D) in the absorbing medium supplied from loop take out sample and detect peroxide content.
priorityDate 2013-01-16^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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