http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-105294628-B
Outgoing Links
Predicate | Object |
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classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07H1-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07H17-07 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D311-30 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D311-40 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07H17-07 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07H1-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D311-40 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D311-30 |
filingDate | 2015-11-11^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2017-07-07^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2017-07-07^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-105294628-B |
titleOfInvention | A kind of method that separation from chrysanthemum indicum prepares flavones ingredient |
abstract | The invention discloses a kind of method that separation from chrysanthemum indicum prepares flavones ingredient.Processing step is:(1) chrysanthemum indicum raw material is crushed, and adds 5 10 times to measure industrial alcohol solution ultrasonic extraction 23 times, and extract solution is concentrated to give medicinal extract;(2) medicinal extract is dissipated with moisture, and respectively with organic solvent-normal hexane, ethyl acetate, extracting n-butyl alcohol, concentration acetic acid ethyl acetate extract obtains crude extract;(3) flavones ingredient (acacetin/robinin in crude extract is isolated and purified with high-speed counter-current chromatograph again, apiolin, cyanidenon, linarin), its two-phase solvent system is n-hexane chloroform methanol water, upper phase is fixing phase, lower phase is mobile phase, and UV-detector on-line monitoring collects each stream part vacuum concentration, crystallization, dries and both obtained.The present invention is simple to operate, and pollution is few. |
priorityDate | 2015-11-11^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
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