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filingDate 2018-06-20^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2021-01-26^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2021-01-26^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-110615736-B
titleOfInvention A kind of preparation method of dicarboxylic acid
abstract The invention discloses a method for preparing a dicarboxylic acid. The method comprises the following steps: 1) subjecting a raw material system containing a cyclic olefin and a monocarboxylic acid to an addition reaction under the action of an addition catalyst to generate a carboxylic acid containing The intermediate product system of the cyclic ester; 2) the intermediate product system is subjected to an epoxidation reaction under the action of an oxidation catalyst to generate a corresponding dicarboxylic acid product. In the diacid synthesis route provided by the application, the single-pass conversion rate of the addition reaction is high, and the selectivity of the corresponding carboxylic acid cyclic ester is good; in the addition-oxidation synthesis route provided by the application, the addition and oxidation reaction rates are both fast , and the corresponding diacid product yield is high. The addition-oxidation synthesis route provided in this application is suitable for continuous, stable and large-scale production of corresponding diacid products.
priorityDate 2018-06-20^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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