http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114994231-A
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_45ef247660b74a66edc2423527e91d7a |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N30-96 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-96 |
filingDate | 2022-06-08^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4723c2932894c5b5b379f3b707987752 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f89b3702aba73fdb100824c9f9ed43f3 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_86d01cd9dcbecb2a49445774019f19d0 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2153cc4e5e414c99c7cb634d6d092df7 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_c41a7bf52725b2470128b93787bbe94e http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_828e5c67ab297bb8790baa99dfba12eb http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_30be41b6f5a3e47f1f73fb2ae19d5d11 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_9786f32252132633a4c1f453c1af5546 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_29a64dc30d09b27c5dd6c8ece3735482 |
publicationDate | 2022-09-02^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-114994231-A |
titleOfInvention | A kind of method for determining nitrite in rifampicin or rifapentine by ion chromatography |
abstract | The invention belongs to the technical field of drug detection, and in particular relates to a method for determining nitrite in rifampicin or rifapentine by ion chromatography, comprising the following steps: taking rifampicin or rifapentine crude drug, passing through methanol and After the diluent composed of deionized water is dissolved, use RP solid phase extraction column to remove impurities, and collect the 6mL of the subsequent filtrate as the test solution for use; take the blank sample diluent, and then add the nitrite standard solution to prepare different concentrations. The reference substance solution is for standby use; carry out the test solution and the reference substance solution of different concentrations under preset ion chromatographic conditions, respectively, make a standard curve according to the detection results of the reference substance solutions of different concentrations, and then according to The standard curve and the test results of the test solution were used to calculate the content of nitrite in the test solution. Using the method provided by the invention to determine the nitrite in rifampicin or rifapentine has good linearity, accuracy, limit of quantification and limit of detection. |
priorityDate | 2022-06-08^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
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