http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-3956285-A1
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_fb78b459e21bb4fd52850a12cab27387 |
classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y02P20-582 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B01J31-0225 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C67-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C67-58 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B01J27-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C67-54 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C69-54 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-54 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-58 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-08 |
filingDate | 2020-04-02^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_aee1ae16bc1b2e0655cd0d781e43219b http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f3ac4d59fb426c0317ed2ab1fda7270c http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_14f500c608c6c72438d5773829b08893 |
publicationDate | 2022-02-23^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | EP-3956285-A1 |
titleOfInvention | Acid catalyzed synthesis of methyl acrylate from acrylic acid and methanol |
abstract | A method for preparing methyl acrylate comprises: a) heating in a reaction zone a mixture comprising acrylic acid, methanol, and an acid catalyst to react and form a reaction product comprising methyl acrylate which is vaporized with other light components and then fed to a distillation zone, wherein a feed stream entering the reaction zone comprises methanol to acrylic acid in a molar ratio of greater than 1 and less than 2, and a residence time in the reaction zone ranges from 0.25 to 2 hours; b) condensing and phase-separating a distillate from the distillation zone to form an organic phase comprising methyl acrylate and an aqueous phase; c) returning a portion of the organic phase to the distillation zone as organic reflux; and d) feeding the remainder of the organic phase and the aqueous phase of the distillation zone to an extraction column to form a methanol rich aqueous effluent and an organic effluent comprising methyl acrylate. |
priorityDate | 2019-04-16^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
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