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filingDate 1978-09-22^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b744aaa941b245ac7fd05044c5f392e2
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publicationDate 1980-03-26^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-S5543017-A
titleOfInvention Preparation of 2-chloro-5-trichloromethylpyridine
abstract NEW MATERIAL:2-chloro-5-trichloromethylpyridine. n USE: Medicines, pesticides, and dyes, particularly herbicides, and intermediates for selective herbicides killing the true grass weeds without doing substantial damage to broad-leaved crops, e.g. cotton and soybean. n PROCESS: One mole of β-picoline is reacted with 4-8mol of chlorine in the gaseous phase in the presence of 5W15mol of an inert diluent gas comprising an inert gas, e.g. nitrogen or helium, a halogenated hydrocarbon, e.g. carbon tetrachloride or trichloroethylene, preferably nitrogen or carbon tetrachloride or their mixture at 250W550°C, preferably 350W500°C, to give the objective compound. The resulting compound can be converted to a 4-(5-trifluoromethylpyridyl-2-oxy) phenoxyalkanecarboxylic acid (a selective herbicide). n COPYRIGHT: (C)1980,JPO&Japio
priorityDate 1978-09-22^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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