Predicate |
Object |
assignee |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_7de9a25822d6b24e133a04bcfcea3c88 http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_e6cccf14f4c6ec9998bf99c0c98074c6 http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_bd5c02153a94d8c9ee5cf4358d39b65d http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_99d1e9e140c45c1c4c28978199dd4070 |
classificationCPCAdditional |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08L2201-54 |
classificationCPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G18-10 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G18-44 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G18-0866 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G18-0823 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G18-4238 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08L75-12 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G18-4854 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G18-18 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G18-6651 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G18-6659 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G18-722 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G18-73 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G18-6685 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G18-6692 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G18-765 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G18-348 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G18-755 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G18-758 |
classificationIPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08L75-12 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G18-66 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G18-75 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G18-76 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G18-72 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G18-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G18-10 |
filingDate |
2017-03-16^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate |
2018-09-18^^<http://www.w3.org/2001/XMLSchema#date> |
inventor |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b89f0078f2984fe086047b22de69fae8 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e8cc9d1d8b63a261c6b7b786f7bd6f40 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f9830c688798b76d1776d0ec5e72948f |
publicationDate |
2018-09-18^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber |
US-10077329-B1 |
titleOfInvention |
Method of producing polyurethane dispersion by solvent free process |
abstract |
A method of producing PUD by a solvent free process includes drying polyol in vacuum; placing the dried polyol and DMBA in a reaction vessel to mix until a first mixture becomes transparent; adding diisocyanate which having functional group of isocyanate (—NCO) to the first mixture to react until —NCO terminated first prepolymer is formed; decreasing temperature of the —NCO terminated first prepolymer to 65° C.; adding a neutralizing agent to the —NCO terminated first prepolymer until —NCO terminated second prepolymer is formed; adding the remaining diisocyanate having isocyanate functional group to the —NCO terminated second prepolymer to form a second mixture; adding deionized water to the second mixture to form prepolymer dispersion; and adding chain extension agent to the prepolymer dispersion to rotate at a range of 200 to 2,000 rpm for chain extension for 1-3 hours until solid content 40.0 wt. % solvent free PUD is produced. |
priorityDate |
2017-03-16^^<http://www.w3.org/2001/XMLSchema#date> |
type |
http://data.epo.org/linked-data/def/patent/Publication |