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publicationDate 2002-03-21^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-2002035230-A1
titleOfInvention Polymerisation reactor and process
abstract A continuous static polymerisation reactor unit for the production of liquid polymers, in particular high viscosity organopolysiloxanes, in a predetermined viscosity range comprises a reactor ( 1 ) a supply means ( 10,25 ) for supplying monomers and/or oligomers to an inlet means ( 2 ), and an outlet means ( 5 ). The inlet means ( 2 ) is adapted for the introduction of a reaction mixture into a reaction chamber ( 3 ), and a means for introducing at least one viscosity controlling agent into the supply means is provided to form a reaction mixture with monomers and/or oligomers ( 11,13,15,12,14,16 ). The unit is adapted to maintain the values of temperature and flow rate of the resulting reaction mixture/polymer in the reaction chamber ( 3 ) substantially constant. A control means ( 24 ) is used to detect any variation from a predetermined pressure drop value between the inlet means ( 2 ) and the outlet means ( 5 ), and should such a variation occur the control means ( 24 ) is also used to compute and control a compensating rate of introduction of one or more of the at least one viscosity controlling agents to cause the pressure drop between the inlet means ( 2 ) and the outlet means ( 5 ) to revert to the predetermined value. A process for making liquid polymers within a predetermined viscosity range is also disclosed.
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