http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-2009114522-A1

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publicationDate 2009-05-07^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-2009114522-A1
titleOfInvention Method of minimizing aldehyde-based impurities in a process stream
abstract Oxidation of an alkane to an alkanone in a process stream forms aldehyde-based impurities. A method of minimizing the aldehyde-based impurities introduces an amine into the process stream to minimize the aldehyde-based impurities. The amine interacts with the alkanone and the aldehyde-based impurities thereby forming heavy products. The method separates the heavy products from the alkanones to reduce a level of the aldehyde-based impurities. The process stream preferably includes cyclohexyl ketone as the alkanone and n-hexanal as the aldehyde-based impurity. The method is typically involved in synthesis of a caprolactam.
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