http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-2009171115-A1

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filingDate 2006-04-05^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2009-07-02^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-2009171115-A1
titleOfInvention Preparation of ion dissociation functional molecule and preparation of raw material molecule thereof
abstract Disclosed is a method of preparing an ion dissociation functional molecule which is chemically and thermally stable under the operating conditions required in an electrochemical system such as a fuel cell and which is suitable for use as a material of, for example, a proton conductor used in a fuel cell, in a higher yield and more easily, more efficiently, more inexpensively and more safely, than by the existing art. In a second step of reacting AgOOCCF 2 SO 2 F with iodine to synthesize a raw material molecule ICF 2 SO 2 F, the reactants mixed in equimolar relation are reacted with each other at 110° C., which is higher than that in the existing art, to thereby enhance the production efficiency of the raw material molecule, then a mixed gas of the thus produced raw material molecule with carbon dioxide is pre-cooled in an exhaust passage kept at −15° C., followed by trapping the raw material molecule by a trapping vessel cooled with dry ice, whereby the trapping efficiency for the raw material molecule is enhanced. In a third step which would be carried out using an autoclave in the existing art, a fullerene and the raw material molecule are reacted by use of a reaction solvent having a boiling point comparable to or higher than the reaction temperature, whereby the reaction is permitted to take place at normal pressure or in a slightly pressurized condition.
priorityDate 2005-05-11^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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