http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-2019127497-A1

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filingDate 2018-09-17^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_c7515459a9ccbcaaf071254f5506575c
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publicationDate 2019-05-02^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-2019127497-A1
titleOfInvention Toluene Free Silica Supported Single-Site Metallocene Catalysts from In-Situ Supported MAO Formation in Aliphatic Solvents
abstract The present disclosure provides a method for preparing a catalyst system comprising contacting in an aliphatic solvent at a temperature of from less than 0° C. to −60° C. at least one support material having absorbed water and at least one hydrocarbyl aluminum compound to form a supported alumoxane (catalyst precursor) and contacting the supported alumoxane with at least one catalyst compound having a Group 3 through Group 12 metal atom or lanthanide metal atom. The supported alumoxane may be heated prior to contact with the catalyst compound.
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