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filingDate 1973-05-24^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1974-12-10^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 1974-12-10^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-3853813-A
titleOfInvention Polyimide precursor and method and composition for preparing it
abstract A composition is disclosed of a dianhydride and a tetracarboxylic acid in the proportions of about 50 to about 70 mole % dianhydride to about 30 to about 50 mole % tetracarboxylic acid, a stoichiometric amount of an aromatic diisocyanate, and a solvent for the dianhydride, the tetracarboxylic acid, and the diisocyanate. A polyimide precursor is prepared by heating the composition at about 30* to 70*C until the evolution of carbon dioxide substantially ceases, and then at about 30* to about 100*C until its viscosity is about Q to about Z6 on the GardnerHoldt viscosity scale at 18% solids. The polyimide precursor can be spread on a substrate and cured to produce a polyimide film or coated on a wire and cured to produce a polyimide wire enamel.
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