http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-4422974-A

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_7c55d2673c544222e80609309a862cf8
classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07J9-00
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07J9-00
filingDate 1982-07-08^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1983-12-27^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d939a969cc6c6d5845ec9723daa72c4c
publicationDate 1983-12-27^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-4422974-A
titleOfInvention Process for the purification of β-sitosterol isolated from the unsaponifiables in crude soap from the sulphate cellulose process
abstract The invention relates to a process for the preparation of beta -sitosterol having a low content of alpha -sitosterol of a sterol mixture isolated from the unsaponifiables obtained from crude soap from the sulphate cellulose process. The invention is based on crystallization of the sterol mixture from a mixture of an organic solvent and water, preferably 1,2-dichloroethylene or methyl ethyl ketone and water. By means of the process according to the invention, from starting materials containing 20 to 25% alpha -sitosterol is obtained a product which contains less than 5% alpha -sitosterol and which, when required, can be retreated by means of the process according to the invention to obtain beta -sitosterol containing less than 1% alpha -sitosterol. When using methyl ethyl ketone as organic solvent, beta -sitosterol is also purified of any betulin contained in the starting material.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-0783514-B2
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-5097012-A
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http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-0783514-A1
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-2004267032-A1
priorityDate 1981-07-21^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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