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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D303-16
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D305-06
filingDate 1989-07-14^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1992-08-04^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_9c0e9224ff298642bdc74b793532ac87
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e1dbb8ac58cdcbed22a7fc755631a415
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a0ba8f35d8dfd54db957246e2b914b4f
publicationDate 1992-08-04^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-5136062-A
titleOfInvention Preparation of epoxy nitrates
abstract A method of preparing a nitrate ester of an epoxy alcohol, which consists of reacting an epoxy alcohol with N 2 O 5 in an inert solvent at a temperature of -10° C. to -40° C., followed by quenching the reaction mixture in aqueous solution. Quenching separates the nitric acid and nitrate ester coproducts into aqueous and organic phases respectively to prevent subsequent reaction between the two. Reaction between the nitric acid coproduct and epoxy alcohol reagent to produce acyclic contaminants is supressed by adding the epoxy alcohol to excess N 2 O 5 , thereby rapidly converting available alcohol to nitrate ester.
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priorityDate 1988-07-22^^<http://www.w3.org/2001/XMLSchema#date>
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