http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-5177267-A

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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C31-20
filingDate 1992-05-22^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1993-01-05^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0b509dc8c6655918f8f3a80788b77962
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_46444c5306eb33e7da1904dcd0b0603c
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publicationDate 1993-01-05^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-5177267-A
titleOfInvention Continuous process for the recovery of 2 ethylhexanal and a tertiary amine from a mixture comprising 2-ethyl-2-(hydroxymethyl) hexanal, 2-ethylhexanal, tertiary amine and water
abstract Disclosed is a continuous process for the manufacture of 2-ethyl-2-(hydroxymethyl)hexanal wherein 2-ethylhexanal, formaldehyde and a tertiary amine are continuously fed to a reaction zone and crude product comprising an aqueous phase and an organic phase containing 2-ethyl-2-(hydroxymethyl)hexanal and 2-ethylhexanal is continuously removed from the reaction zone. Also disclosed are processes for (1) the azeotropic distillation of the organic phase of the crude product whereby unreacted 2-ethylhexanal is recovered and (2) the catalytic hydrogenation of the refined, organic phase of the crude product to produce 2-butyl-2-ethyl-1,3-propanediol.
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priorityDate 1991-07-25^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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