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filingDate 1998-05-19^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2000-01-04^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2000-01-04^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-6011131-A
titleOfInvention Process for the preparation of polyamides
abstract Process for the preparation of polyamides comprising the steps of A) reacting a soybean oil condensate obtained from the deodorization of refined soybean oil and which contains less than 30% by weight of free and esterified oleic acid based on the total weight of free and esterified fatty acids in said condensate, with a C 1-4 alkanol in the presence of a zinc oxide catalyst to convert free fatty acids and fatty acid glyceride esters to fatty acid C 1-4 alkyl esters; n B) removing excess C 1-4 alkanol, volatile reaction by-products, water, and the zinc oxide catalyst from the resulting reaction mixture; n C) heating the reaction mixture from step B) under vacuum to obtain a distillate of fatty acid C 1-4 alkyl esters; n D) separating the distillate from step C) into a fraction containing mostly C 16-18 saturated fatty acid C 1-4 alkyl esters and a second fraction containing mostly C 16-18 unsaturated fatty acid C 1-4 alkyl esters wherein the oleic acid C 1-4 alkyl ester content is less than about 35% by weight thereof; n E) dimerizing said second fraction in the presence of montmorillonite clay; and n F) reacting the dimerized second fraction with a polyamine.
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