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filingDate 2005-08-26^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2008-12-16^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_596062ef20fa80f44419ebb77c3fc5c0
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publicationDate 2008-12-16^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-7465842-B2
titleOfInvention Enantioselective biotransformation for preparation of protein tyrosine kinase inhibitor intermediates
abstract The invention relates to biocatalytic methods for preparing enantiomerically pure stereoisomers of 1-(2,6-dichloro-3-fluorophenyl)ethanol. Disclosed are methods of preparation of the desired (S)-enantiomer, which methods are based on a combination of enzymatic resolution, chemical esterification and chemical hydrolysis with inversion of 1-(2,6-dichloro-3-fluorophenyl)ethyl esters or stereoselective bio-reduction of 2,6-dichloro-3-fluoro-acetophenone with a biocatalyst such as an enzyme or a microorganism. The chiral (S)-enantiomer can be used in the synthesis of certain enantiomerically enriched, ether linked 2-aminopyridine compounds that potently inhibit auto-phosphorylation of human heptocyte growth factor receptor.
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http://rdf.ncbi.nlm.nih.gov/pubchem/compound/CID45073502
http://rdf.ncbi.nlm.nih.gov/pubchem/protein/ACCQ7CSM1
http://rdf.ncbi.nlm.nih.gov/pubchem/protein/ACCQ0DWH1
http://rdf.ncbi.nlm.nih.gov/pubchem/gene/GID1252153
http://rdf.ncbi.nlm.nih.gov/pubchem/gene/GID32114
http://rdf.ncbi.nlm.nih.gov/pubchem/substance/SID419589679
http://rdf.ncbi.nlm.nih.gov/pubchem/protein/ACCP19835
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http://rdf.ncbi.nlm.nih.gov/pubchem/taxonomy/TAXID5418
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http://rdf.ncbi.nlm.nih.gov/pubchem/protein/ACCA0A486WWU7
http://rdf.ncbi.nlm.nih.gov/pubchem/protein/ACCP20368
http://rdf.ncbi.nlm.nih.gov/pubchem/gene/GID3082
http://rdf.ncbi.nlm.nih.gov/pubchem/gene/GID6481678
http://rdf.ncbi.nlm.nih.gov/pubchem/substance/SID453447712
http://rdf.ncbi.nlm.nih.gov/pubchem/protein/ACCP20369
http://rdf.ncbi.nlm.nih.gov/pubchem/protein/ACCQ5AR48
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http://rdf.ncbi.nlm.nih.gov/pubchem/gene/GID4023
http://rdf.ncbi.nlm.nih.gov/pubchem/taxonomy/TAXID5081
http://rdf.ncbi.nlm.nih.gov/pubchem/protein/ACCP23916
http://rdf.ncbi.nlm.nih.gov/pubchem/protein/ACCJ3SDX8
http://rdf.ncbi.nlm.nih.gov/pubchem/substance/SID142299414
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http://rdf.ncbi.nlm.nih.gov/pubchem/substance/SID230882103
http://rdf.ncbi.nlm.nih.gov/pubchem/substance/SID226417492
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http://rdf.ncbi.nlm.nih.gov/pubchem/taxonomy/TAXID5535
http://rdf.ncbi.nlm.nih.gov/pubchem/protein/ACCQ7U1B9
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http://rdf.ncbi.nlm.nih.gov/pubchem/protein/ACCQ5HRD6
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http://rdf.ncbi.nlm.nih.gov/pubchem/protein/ACCI6L6E1
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http://rdf.ncbi.nlm.nih.gov/pubchem/protein/ACCQ9AB15
http://rdf.ncbi.nlm.nih.gov/pubchem/gene/GID40267
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http://rdf.ncbi.nlm.nih.gov/pubchem/protein/ACCP28474
http://rdf.ncbi.nlm.nih.gov/pubchem/protein/ACCQ9VG48
http://rdf.ncbi.nlm.nih.gov/pubchem/gene/GID946260
http://rdf.ncbi.nlm.nih.gov/pubchem/protein/ACCQ7CTQ3
http://rdf.ncbi.nlm.nih.gov/pubchem/protein/ACCP28469
http://rdf.ncbi.nlm.nih.gov/pubchem/protein/ACCQ7CU70
http://rdf.ncbi.nlm.nih.gov/pubchem/protein/ACCP23991
http://rdf.ncbi.nlm.nih.gov/pubchem/protein/ACCP28483
http://rdf.ncbi.nlm.nih.gov/pubchem/taxonomy/TAXID1593383
http://rdf.ncbi.nlm.nih.gov/pubchem/protein/ACCQ9KR28
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http://rdf.ncbi.nlm.nih.gov/pubchem/taxonomy/TAXID5141
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http://rdf.ncbi.nlm.nih.gov/pubchem/gene/GID5144186

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