http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-8586241-B2

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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01B25-30
filingDate 2009-08-25^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2013-11-19^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0208f6d5af5f4c017c72b116533a3457
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publicationDate 2013-11-19^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-8586241-B2
titleOfInvention Synthesis of LIFEPO4 under hydrothermal conditions
abstract The present invention relates to a process for the preparation of compounds of general Formula (I) L a-b M 1 b Fe 1-c M 2 c P d-e M 3 e O x (I), wherein Fe has the oxidation state +2 and M 1 , M 2 , M 3 , a, b, c, d, e and x are: M 1 : Na, K, Rb and/or Cs, M 2 : Mn, Mg, Al, Ca, Ti, Co, Ni, Cr, V, M 3 : Si, S, F a: 0.8-1.9, b: 0-0.3, c: 0-0.9, 15 d: 0.8-1.9, e: 0-0.5, x: 1.0-8, depending on the amount and oxidation state of Li, M 1 , M 2 , P, M 3 , wherein compounds of general Formula (I) are neutrally charged, comprising the following steps (A) providing a mixture comprising at least one lithium-comprising compound, at least one iron-comprising compound, in which iron has the oxidation state +3, and at least one M 1 -comprising compound, if present, and/or at least one M 2 -comprising compound, if present, and/or least one M 3 -comprising compound, if present, and at least one reducing agent which is oxidized to at least one compound comprising at least one phosphorous atom in oxidation state +5, and (B) heating the mixture obtained in step (A) at a temperature of 100 to 500° C. and at an autogeneous pressure to reduce Fe to oxidation state +2 and to obtain a compound of general Formula (I).
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priorityDate 2008-08-26^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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