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filingDate 2011-10-14^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2015-03-03^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ea145c76ad7d5b60fdde4a83941beac5
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publicationDate 2015-03-03^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-8969550-B2
titleOfInvention Process for the synthesis of cyclic carbamates
abstract The invention is directed to a process for the preparation of a cyclic carbamate starting with o-aminobenzyl alcohol and/or a suitable salt thereof, which is reacted with a cyclization agent selected from phosgene, diphosgene, triphosgene and mixtures thereof, and in that the reaction carried out in the presence of an aqueous base, and a water-immiscible organic solvent, said organic solvent mainly comprising at least one compound selected from C 2-5 -alkyl C 2-5 -carboxylates and mixtures of at least one C 2-5 -alkyl C 2-5 -carboxylate with at least one C 5-8 -alkane.
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