http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-2013091381-A1

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filingDate 2012-08-02^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_174a7cd48f5e792b207afb1fbdfe773d
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publicationDate 2013-06-27^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber WO-2013091381-A1
titleOfInvention Preparation method for polytetrafluoroethylene resin with high fluorine content
abstract Provided is a preparation method for polytetrafluoroethylene resin with high fluorine content. The method comprises: adding a solvent, liquid nonfluorine comonomers and an initiator to a reaction kettle; evacuating the oxygen from the reacting system under vacuum condition; controlling the polymerization reaction temperature in a range of 60 to 75℃; feeding the tetrafluoroethylene monomer in gas phase; adding the additional tetrafluoroethylene monomer and the initiator continuously or intermittently during the polymerization reaction with a reaction time of 17 to 21 hours. The reaction kettle for conducting said preparation method is also provided. Medium viscosity media is suitable for the present invention, and the reaction kettle equipped with a special cylinder stirrer is utilized under limited stirring speed for allowing tetrafluoroethylene type normal temperature cured resin with high fluorine content to be prepared well.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-112058200-A
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